Test |
Monograph |
Limits |
Typical Lot Analysis |
Assay (corrected for water), min |
ACS |
99.5% |
99.9% |
Assay (anhydrous basis), min |
NF |
99.0% |
99.7% |
Appearance |
ACS |
Clear liquid w/characteristic odor |
Pass |
Identification (IR) |
NF |
Conforms to infrared spectra |
Pass |
Identification test B(GC) |
NF |
Conforms to Reference Chromatogram |
Pass |
Specific Gravity @ 25°C, max |
NF |
0.7890 |
0.787 |
Color (APHA), max |
ACS |
10 |
<10 |
Residue After Evaporation, max |
ACS |
10ppm |
<10ppm |
Non-Volatile Residue, max |
NF |
0.004% |
<0.001% |
Readily Oxidizable Substances |
NF |
Color not completely disappear in 15min. |
Pass |
Substances Reducing KMnO4 |
ACS |
Pass |
Solubility In Water |
ACS |
Solution remains clear for 30min. |
Pass |
Titrable Acid, max |
ACS |
0.0003meq/g |
0.0002meq/g |
Titrable Base, max |
ACS |
0.0006meq/g |
0.0001meq/g |
Aldehyde (as HCHO), max |
ACS |
0.002% |
<0.002% |
IPA, max |
ACS |
0.05% |
0.001% |
Methanol, max |
ACS |
0.05% |
0.03% |
Water, max |
NF |
0.5% |
0.30% |